Freezing behaviour and spray freeze granulation drying of silicon nitride slurries prepared from tert-butyl alcohol and cyclohexane solvent mixtures

Riko Yamazaki; Junichi Tatami; Motoyuki Iijima; Shinya Kawaguchi; Naoki Kondo

doi:10.1016/j.apt.2025.105030

journal article Open Access Nov 01, 2025

Freezing behaviour and spray freeze granulation drying of silicon nitride slurries prepared from tert-butyl alcohol and cyclohexane solvent mixtures

Riko Yamazaki Junichi Tatami

Motoyuki Iijima Shinya Kawaguchi

Naoki Kondo

Advanced Powder Technology Vol. 36 No. 11 pp. 105030 · Elsevier BV

View at Publisher Save 10.1016/j.apt.2025.105030

Topics

No keywords indexed for this article. Browse by subject →

References

25

[1]

Sultana "Exploring conventional and emerging dehydration technologies for slurry/liquid food matrices and their impact on porosity of powders: a comprehensive review" Compr. Rev. Food Sci. Food Saf. (2024) 10.1111/1541-4337.13347

[2]

Chua "Evaluating spray gelation and spray freeze drying as the granulation method to prepare oral tablets of amorphous drug nanoplex" Adv. Powder Technol. (2023) 10.1016/j.apt.2023.104151

[3]

Geng "Formation mechanism and control of a large-scale lamellar structure in freeze-cast Al2O3 ceramics under dual temperature gradients" J. Eur. Ceram. Soc. (2018) 10.1016/j.jeurceramsoc.2018.01.039

[4]

Liu "Tunable pore size and microstructure of hierarchical porous silica ceramics by freeze casting method using dual solvent as a template" J. Eur. Ceram. Soc. (2024) 10.1016/j.jeurceramsoc.2024.01.074

[5]

Lasalle "Particle redistribution and structural defect development during ice templating" Acta Mater. (2012) 10.1016/j.actamat.2012.02.023

[6]

Kondo "Lowering compaction pressure and sintering temperature of alumina using spray freeze granulation dried granules" J. Ceram. Soc. Jpn. (2025) 10.2109/jcersj2.24086

[7]

Kuzmin "Morphology of alumina granules obtained by spray freeze drying with twin-fluid atomization" Int. J. Appl. Ceram. Technol. (2021) 10.1111/ijac.13802

[8]

Uchida "Spray-Freeze-Dried Granules for Ceramics Fabrication: American Ceramic Society Bulletin" Am. Ceram. Soc. Bull. (2002)

[9]

Olhero "Thermodynamic Studies on the AlN Sintering Powders Treated with Phosphate Species" J. Am. Ceram. Soc. (2007) 10.1111/j.1551-2916.2007.01922.x

[10]

Morisada "A New Water-Resistant Coating for AlN Powders" Int. J. Appl. Ceram. Technol. (2004) 10.1111/j.1744-7402.2004.tb00188.x

[11]

Yamazaki "Effect of Graphene Coating by Mechanical Treatment on Water Resistance of Aluminum Nitride Particles" Funtai Kogakkaishi (2024) 10.4164/sptj.61.154

[12]

da Rosa Braun "Impact of a tert-butyl alcohol-cyclohexane system used in unidirectional freeze-casting of SiOC on compressive strength and mass transport" Materials & Design 212 (2021) 10.1016/j.matdes.2021.110186

[13]

Donius "Cryogenic EBSD reveals structure of directionally solidified ice–polymer composite" Mater Charact (2014) 10.1016/j.matchar.2014.04.003

[14]

Dedovets "Multiphase imaging of freezing particle suspensions by confocal microscopy" J. Eur. Ceram. Soc. (2018) 10.1016/j.jeurceramsoc.2018.01.045

[15]

Deville "In Situ X-Ray Radiography and Tomography Observations of the Solidification of Aqueous Alumina Particle Suspensions—Part I: initial Instants" J. Am. Ceram. Soc. (2009) 10.1111/j.1551-2916.2009.03163.x

[16]

Iijima "Operando observation of concentrated SiO2 suspensions by optical coherent tomography during flow curve measurements: the relationship between polymer dispersant structures and surface interactions" J. Colloid Interface Sci. (2022) 10.1016/j.jcis.2021.08.125

[17]

Kuroda "Novel operando observation technique based on combined optical coherence tomography–thermogravimetry for monitoring internal structural changes of drying ceramic slurries" J. Ceram. Soc. Japan (2023) 10.2109/jcersj2.23008

[18]

Takahashi "In-situ Observation of Change Process in Void Morphology in Powder Bed under Uniaxial Pressing of Al2O3 Granules by Optical Coherence Tomography" J. Jpn. Soc. Powder Powder Metallurgy (2020) 10.2497/jjspm.67.615

[19]

Sakamoto "Prediction of strength based on defect analysis in Al2O3 ceramics via non-destructive and three-dimensional observation using optical coherence tomography" J. Ceram. Soc. Japan (2019) 10.2109/jcersj2.19020

[20]

Iijima "Polyethyleneimine–Oleic Acid complex as a Polymeric Dispersant for Si3N4 and Si3N4-based Multicomponent Nonaqueous Slurries" Ind. Eng. Chem. Res. (2015) 10.1021/acs.iecr.5b03696

[21]

Uematsu "Infrared Microscopy for Examination of Structure in Spray-Dried Granules and Compacts" J. Am. Ceram. Soc. (2001) 10.1111/j.1151-2916.2001.tb00646.x

[22]

Leo "Freeze casting for near-net-shaping of dense zirconium diboride ceramics" J. Am. Ceram. Soc. (2018) 10.1111/jace.15451

[23]

Hyun "Synthesis of low-k porous silica films via freeze drying" J. Mater. Sci. Lett. (2000) 10.1023/a:1006775213914

[24]

Controlling the morphology of ceramic and composite powders obtained via spray drying – A review

Agnese Stunda-Zujeva, Zilgma Irbe, Liga Berzina-Cimdina

Ceramics International 2017 10.1016/j.ceramint.2017.05.023

[25]

Bai "Bioinspired large-scale aligned porous materials assembled with dual temperature gradients" Sci. Adv. (2015) 10.1126/sciadv.1500849

Cited By

2

Correlation analysis of granulation condition, granule properties and green density of alumina ceramics fabricated by spray freeze granulation drying

Ying Chung, Naoki Kondo · 2026

Advanced Powder Technology

Metrics

2

Citations

25

References

Details

Published: Nov 01, 2025
Vol/Issue: 36(11)
Pages: 105030
License: View

Authors

Yokohama National University

Department of Gastroenterology Ise Red Cross Hospital Ise Japan

N

Naoki Kondo

Funding

Japan Society for the Promotion of Science Award: 22H00257

Hosokawa Powder Technology Foundation Award: HPTF23504

Cite This Article

Riko Yamazaki, Junichi Tatami, Motoyuki Iijima, et al. (2025). Freezing behaviour and spray freeze granulation drying of silicon nitride slurries prepared from tert-butyl alcohol and cyclohexane solvent mixtures. Advanced Powder Technology, 36(11), 105030. https://doi.org/10.1016/j.apt.2025.105030

Freezing behaviour and spray freeze granulation drying of silicon nitride slurries prepared from tert-butyl alcohol and cyclohexane solvent mixtures

You May Also Like