A Polar Luminescent Zn Polymer Containing an Unusual Noninterpenetrated utp Net

Jian Zhang; Yu-Biao Chen; Shu-Mei Chen; Zhao-Ji Li; Jian-Kai Cheng; Yuan-Gen Yao

doi:10.1021/ic060276t

journal article Mar 24, 2006

A Polar Luminescent Zn Polymer Containing an Unusual Noninterpenetrated utp Net

Jian Zhang

Yu-Biao Chen Shu-Mei Chen Zhao-Ji Li Jian-Kai Cheng Yuan-Gen Yao

Inorganic Chemistry Vol. 45 No. 8 pp. 3161-3163 · American Chemical Society (ACS)

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A mixture of ZnSO4·7H2O (0.287 g, 1.0 mmol), BPP (0.198 g, 1.0 mmol), benzene-1,3,5-tricarboxylate acid (0.105 g, 0.5 mmol) with NaOH (0.040 g, 1.0 mmol), and 15 mL of water was placed in a Parr Teflon-lined stainless steel vessel (25 cm3), and then the vessel was sealed and heated to 160 °C. The temperature was held for 3 days, and then the reactant mixture was cooled at a rate of 0.5 °C min-1to lead to the formation of colorless crystals of1(yield = about 35% based on Zn; final pH = 5.2). Anal. Calcd for1: C, 53.95; H, 4.12; N, 5.72. Found: C, 53.99; H, 4.22; N, 5.69. IR (solid KBr pellet, v/cm-1) for complex1: 3419 (m), 1633 (vs), 1567 (m), 1435 (s), 1366 (s), 1227 (m), 1099 (w), 1030(m), 767 (s), 718 (s), 615 (w).

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Published: Mar 24, 2006
Vol/Issue: 45(8)
Pages: 3161-3163

Authors

J

Jian Zhang