Growth and characterization of 6-chloro-2,4-dinitroaniline crystals in anti-solvent precipitation and reprecipitation methods

Rajaboopathi Mani; Krishnakumar Varadharajan; Marjatta Louhi-Kultanen

doi:10.1039/c3ce42634c

journal article Jan 01, 2014

Growth and characterization of 6-chloro-2,4-dinitroaniline crystals in anti-solvent precipitation and reprecipitation methods

Rajaboopathi Mani

Krishnakumar Varadharajan Marjatta Louhi-Kultanen

CrystEngComm Vol. 16 No. 20 pp. 4183-4193 · Royal Society of Chemistry (RSC)

View at Publisher Save 10.1039/c3ce42634c

Abstract

A superstructure was formed on form I of 6-chloro-2, 4-dinitroaniline crystals. It was observed using a slow evaporation solution growth technique and crystals grown from slow evaporation of the filtrate in anti-solvent precipitation. The thickness of 2D petals in the superstructure is about 100 nm.

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References

37

[1]

Brown Cryst. Growth Des. (2011) 10.1021/cg1011988

[2]

Bag CrystEngComm (2012) 10.1039/c2ce25100k

[3]

Doki J. Chem. Eng. Jpn. (2002) 10.1252/jcej.35.1099

[4]

Kasai Jpn. J. Appl. Phys. (1992) 10.1143/jjap.31.l1132

[5]

Holmback J. Cryst. Growth (1999) 10.1016/s0022-0248(98)01027-6

[6]

Yu J. Cryst. Growth (2005) 10.1016/j.jcrysgro.2005.02.050

[7]

Kitamura Cryst. Growth Des. (2000) 10.1021/cg050635f

[8]

Colfen Angew. Chem., Int. Ed. (2005) 10.1002/anie.200500496

[9]

Su J. Mater. Chem. (2010) 10.1039/c0jm00110d

[10]

Burton Philos. Trans. R. Soc. London, Ser. A (1951) 10.1098/rsta.1951.0006

[11]

Gong Cryst. Growth Des. (2006) 10.1021/cg060133h

[12]

Sun CrystEngComm (2012) 10.1039/c2ce06335b

[13]

Gua J. Alloys Compd. (2011) 10.1016/j.jallcom.2010.11.078

[14]

Zhang Mater. Res. Bull. (2012) 10.1016/j.materresbull.2012.03.038

[15]

Yang J. Colloid Interface Sci. (2012) 10.1016/j.jcis.2011.09.061

[16]

Penn Geochim. Cosmochim. Acta (1999) 10.1016/s0016-7037(99)00037-x

[17]

Helmut Angew. Chem., Int. Ed. (2005) 10.1002/anie.200500496

[18]

Nakanishi Small (2007) 10.1002/smll.200700647

[19]

Wang Langmuir (2009) 10.1021/la8038494

[20]

Self-assembly and application of diphenylalanine-based nanostructures

Xuehai Yan, Pengli Zhu, Junbai Li

Chemical Society Reviews 2010 10.1039/b915765b

[21]

Reddy Chem. Commun. (2005) 10.1039/b500712g

[22]

Krishnakumar J. Therm. Anal. Calorim. (2014) 10.1007/s10973-013-3181-5

[23]

Yu Thermochim. Acta (2013) 10.1016/j.tca.2012.10.023

[24]

Mercury CSD 2.0– new features for the visualization and investigation of crystal structures

Clare F. Macrae, Ian J. Bruno, James A. Chisholm et al.

Journal of Applied Crystallography 2008 10.1107/s0021889807067908

[25]

Wishkerman CrystEngComm (2006) 10.1039/b515447b

[26]

Findlay J. Pharm. Biomed. Anal. (1998) 10.1016/s0731-7085(97)00058-7

[27]

Etter Acc. Chem. Res. (1990) 10.1021/ar00172a005

[28]

Donahue Am. Pharm. Rev. (2011)

[29]

G. Socrates , Infrared and Raman Characteristic Group Frequencies , John Wiley & Sons , England , 3rd edn, 2001

[30]

Lakshmaiah J. Raman Spectrosc. (1989) 10.1002/jrs.1250200709

[31]

Hoghes J. Chem. Soc. A (1971) 10.1039/j19710002181

[32]

Margoshes Spectrochim. Acta (1955)

[33]

Colfen Angew. Chem., Int. Ed. (2005) 10.1002/anie.200500496

[34]

A. A. Chernov , P. N.Segre and A. M.Holmes , in Crystallization Physics in Biomacromolecular Solutions , ed. G. Muller , J.-J. Metois and P. Rudolph , Elsevier , Amsterdam , 1st edn, 2004 , ch. 1, p. 109

[35]

Zhao Adv. Mater. (2008) 10.1002/adma.200800604

[36]

Wohlrab Chem.–Eur. J. (2005) 10.1002/chem.200400420

[37]

Colfen Angew. Chem., Int. Ed. (2003) 10.1002/anie.200200562

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Details

Published: Jan 01, 2014
Vol/Issue: 16(20)
Pages: 4183-4193

Authors

R

Rajaboopathi Mani

Department of Chemical Technology; Lappeenranta University of Technology; Lappeenranta 53851, Finland; Department of Physics; Periyar University

K

Krishnakumar Varadharajan

Department of Physics; Periyar University; Salem 636 011, India

M

Marjatta Louhi-Kultanen

Department of Chemical Technology; Lappeenranta University of Technology; Lappeenranta 53851, Finland

Cite This Article

Rajaboopathi Mani, Krishnakumar Varadharajan, Marjatta Louhi-Kultanen (2014). Growth and characterization of 6-chloro-2,4-dinitroaniline crystals in anti-solvent precipitation and reprecipitation methods. CrystEngComm, 16(20), 4183-4193. https://doi.org/10.1039/c3ce42634c

Growth and characterization of 6-chloro-2,4-dinitroaniline crystals in anti-solvent precipitation and reprecipitation methods

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